The 11-dehydro TXB2 Quant-PAK has been designed for the convenient, precise quantification of 11-dehydro TXB2 by GC- or LC-MS. It includes a 50 μg vial of 11-dehydro TXB2-d4 and a precisely weighed vial of unlabeled 11-dehydro TXB2, with the precise weight (2-4 mg) indicated on the vial. This unlabeled 11-dehydro TXB2 can be used to quantify the 11-dehydro TXB2-d4 standard by constructing a standard curve of peak intensity ratios (deuterated versus unlabeled).